Table I.

13C-NMR data for disinapoyl Glc derived from the usual array of 1D and 2D experiments, and comparison (assigned here) with prior data (Strack et al., 1984)

Ac, Acetone-D6; *, data from Strack et al. (1984).

δ Carbonδ MeODδ Ac/D2Oδ* MeOD
194.293.294.1
274.473.574.4
376.275.276.1
471.470.871.4
579.378.579.2
662.461.862.4
S1 sinapoyl unit
    1126.3125.3126.4
    2/6107.3106.9107.3
    3/5149.6148.5149.5
    4140.3139.7140.2
    7149.1148.3149.0
    8114.7114.2114.7
    9167.4166.1167.1
    3/5-OMe56.956.556.9
S2 sinapoyl unit
    1126.7125.7126.6
    2/6107.1106.6107.1
    3/5149.6148.7149.5
    4139.8139.3139.9
    7148.0146.9147.8
    8115.7115.2115.6
    9168.6166.9168.3
    3/5-OMe56.956.556.9